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Diffraction Diagram

Fig.1 Examples of electron diffraction diagrams recorded under frozen wet conditions from crystals rotated about their long axis. The indexations and the corresponding zone axes of these diagrams are also presented.

(a)The goniometer setting was (a) 36°, (b) -10° (c) +20°.

*Permission Pending for Diffraction Diagrams

Diffraction Diagram

Fig.1 Examples of electron diffraction diagrams recorded under frozen wet conditions from crystals rotated about their long axis. The indexations and the corresponding zone axes of these diagrams are also presented.

(a)The goniometer setting was (a) 36°, (b) -10° (c) +20°.

Fig.2 Examples of electron diffraction diagrams recorded under frozen wet conditions from crystals rotated about an axis perpendicular to their long direction. In (a) reflection 2 is twice as intense as that in 1. In (b) reflection 3 is slightly less intense than 1, 2 and 3 which index as --1-2-1 and --1 2-1 in an orthorhombic system, should have equivalent intensities. This is not the case and hence the monoclinic indexation is favoured.

*Permission Pending for Diffraction Diagrams